Solid State NMR and Materials Applications at High Magnetic Field

Workshop at National High Magnetic Field Laboratory

March 12-13, 2004

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THURSDAY, MARCH 11

5:00pm-8:00pm Registration and Reception (Double Tree Hotel)

FRIDAY, MARCH 12

8:00am-8:45am Continental Breakfast

8:45am-9:00am Welcome and Opening Remarks, Naresh Dalal, Chemistry Chair/FSU

Disorder Systems and Glasses
(Chair: Gina Hoatson)

9:00am-9:30am Measuring Correlated Structure Distributions in Silicate Glasses with 17O NMR.
P. J. Grandinetti, T. Clark, P. Florian, S. Sen, R. Youngman, and J.F. Stebbins

9:30am-10:00am Quasi high resolution 63Cu NMR in dilute Al(Cu) and Al(Cu,Mg) alloys. T.J.Bastow

10:00am-10:30am Solid-state NMR Studies of Oxide Glasses with Unusual Optical Properties.
Josef W. Zwanziger, Joanna L. Shaw, Ulrike Werner-Zwanziger and Robert T. Hart

10:30am-11:00am Coffee Break

Methods
(Chair: Philip Grandinetti)

11:00am-11:30pm The utility of accurate NMR parameter calculations as an aid to NMR at high field.
Ian Farnan, Laurent LePollès, Sharon E. Ashbrook, Miguel Pruneda, Chris J. Pickard, Francesco Mauri

11:30am-12:00pm Heteronuclear correlation NMR spectroscopy of quadrupolar spins; applications to heterogeneous catalysis. M. Pruski

12:00pm-12:30pm Quadrupole Central-Transition (QCT) Spectroscopy at High Magnetic Fields: Blurring the Distinction between Solution and Solid States. Gang Wu

12:30pm-1:15pm Lunch

Catalyst and Zeolite
(Chair: Dominique Massiot)

1:15pm-1:45pm 27Al High Field NMR studies on Zeolites. Ernst R.H. van Eck, Arno P. M. Kentgens

1:45pm-2:15pm Identification of Preferred Al Sites in Zeolites by Solid State NMR at High Magnetic Fields. Oc Hee Han, Seen Ae Chae and S. B. Hong

2:15pm-2:45pm High-field 95Mo MAS NMR of hydrotreatment catalysts precursors.
J.-B. d’Espinose de Lacaillerie, B. Bresson, P. Fonollosa and Zhehong Gan

2:45pm-3:15pm Coffee Break

High Magnetic Fields
(Chair: Zhehong Gan)

3:15pm-3:45pm Structural diagnostic of inorganic materials at different magnetic fields.
D.Massiot, C.Morais, V.Montouillout, F.Fayon, P.Florian, D.Neuville, L.Cormier, N.Sadiki and J.P.Coutures

3:45pm-4:15pm 18 and 40 Tesla 27Al MAS NMR of Methylaluminoxane (MAO). Les Butler

4:15pm-4:45pm Examples of the Applications of High Field NMR of Quadrupole Nuclei to the Characterisation of Materials. Mark E. Smith

4:45pm-6:00pm NHMFL tour

6:00pm-7:00pm Dinner

SATURDAY, MARCH 13

8:15am-9:00am Continental Breakfast

Other Materials
(Chair: Naresh Dalal)

9:00am-9:30am Multinuclear MAS NMR Studies of Perovskite Relaxor Ferroelectrics.
Gina L. Hoatson, William J. Brouwer, Robert L. Vold* and Donghua Zhou*

9:30am-10:00am Asymmetries of local As sites in Asx(S/Se) 1-x glassy and polycrystalline compositions by high field NMR techniques.
Parameswar Hari, Craig Taylor, Phil Kuhns, Bill Moulton and Neil Sullivan

10:00am-10:30am NMR Detection of Structure and Dynamics of Metallic Glasses and Supercooled Liquids. Yue Wu

10:30am-11:00am Coffee Break

Special Session

11:00am-11:30pm MAS Probe Technology for High-Field Multiple Resonance. David Rice, John Stringer

11:30am-12:30pm Topics:
Technology, instrumentation, high magnetic fields and NHMFL

12:30pm Adjourn and Lunch