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Compact TXLine 1H/X Broadband Probe
for 900 MHz UWB magnet


900 MHz 1H/X broadband probe.

1. DESCRIPTION

This 1H/X broadband transmission line probe is operating in NHMFL's new 900 MHz ultra-wide bore magnet, which became operational in August 2004. The new probe utilizes advantages of compact transmission line design which we developed for high frequency magnets. High field magnets are physically long and present challenge for conventional transmission line probes, where RF circuit is mounted outside the magnet. RF losses in Tx line would accumulate very fast over several wavelengths from magnet's bottom to its sweet spot. In our 900 MHz magnet, this distance is almost 5 wavelengths at proton frequency. To avoid unnecessary losses, entire transmission line design is compacted within 7" of space in probe head. Parts of transmission line are responsible for transmitting power to the coil, isolating channels, and balancing the RF circuit for better RF homogeneity. The compact design results in probe with light weight and with higher efficiency of low-frequency X channel.

Similar, 3.2mm broadband MAS probe is being built for the 900 MHz magnet this year.

2. FEATURES

  • Compact TXL design
  • Both channels are balanced for RF homogeneity
  • Interchangeable sample coils — see tuning guide below
  • X nuclei switch in the bottom of the probe
  • Biological range VT capability

    3. EXAMPLE SPECTRA

    Structural and functional studies of ion channels in gramicidin A and study of carbonyl sites in peptides by means of 17O solid-state NMR spectroscopy can be viewed on this page.

    4. TUNING GUIDE

     4 mm ID solenoid 15N 17O
     Bottom insert  16.5 pF (2x33pF in series) 11 pF (2x22pF in series)
     Top chip  none 47 pF
     7x5x12 mm flat coil 15N 17O
     Bottom insert    11 pF (2x22pF in series)
     Top chip    47 pF
     5x7x12 mm vertical flat coil 15N 17O
     Bottom insert    16.5 pF (2x33pF in series)
     Top chip    47 pF
    *Note: 11 pF insert is comprised of two 22 pF chips in series, 16.5 pF - of two 33 pF chips in series.