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 900 MHz 1H/X broadband probe. |
1. DESCRIPTION
This 1H/X broadband transmission line probe is operating in NHMFL's new 900 MHz
ultra-wide bore magnet, which became operational in August 2004.
The new probe utilizes advantages of compact transmission line design which we developed for high frequency magnets.
High field magnets are physically long and present challenge for conventional transmission line probes,
where RF circuit is mounted outside the magnet. RF losses in Tx line would accumulate very fast over several wavelengths
from magnet's bottom to its sweet spot. In our 900 MHz magnet, this distance is almost 5 wavelengths at proton frequency.
To avoid unnecessary losses, entire transmission line design is compacted within 7" of space in probe head. Parts of
transmission line are responsible for transmitting power to the coil, isolating channels, and balancing the RF circuit for
better RF homogeneity. The compact design results in probe with light weight and with higher efficiency of low-frequency X channel.
Similar, 3.2mm broadband MAS probe is being built for the 900 MHz magnet this year.
2. FEATURES
Compact TXL design
Both channels are balanced for RF homogeneity
Interchangeable sample coils see tuning guide below
X nuclei switch in the bottom of the probe
Biological range VT capability
3. EXAMPLE SPECTRA
Structural and functional studies of ion channels in gramicidin A
and study of carbonyl sites in peptides
by means of 17O solid-state NMR spectroscopy can be viewed on this page.
4. TUNING GUIDE
| 4 mm ID solenoid |
15N |
17O |
| Bottom insert |
16.5 pF (2x33pF in series) |
11 pF (2x22pF in series) |
| Top chip |
none |
47 pF |
| 7x5x12 mm flat coil |
15N |
17O |
| Bottom insert |
|
11 pF (2x22pF in series) |
| Top chip |
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47 pF |
| 5x7x12 mm vertical flat coil |
15N |
17O |
| Bottom insert |
|
16.5 pF (2x33pF in series) |
| Top chip |
|
47 pF |
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*Note: 11 pF insert is comprised of two 22 pF chips in series, 16.5 pF - of two 33 pF chips in series.
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