NMR Program - Solid State NMR

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Specs

Designation: Solid State NMR
Location: Tallahassee
Field: 14.1 Tesla
Bore size = 89 mm
Homogeneity = 1 ppb
RT Shims: Bruker Instruments
RT Shims ID = 72 mm
Bruker DRX console with solid state NMR capabilities
Built-in VT controller by Bruker
Amplifiers: Up to 1 kW on all 3 channels

Commercial probes

Bruker ¹H—X—Y triple resonance 4mm MAS probe
Bruker ¹H—X—Y triple resonance 2.5mm MAS probe

NHMFL Low-E probes for biological solids

¹⁵N—¹H static low-E probe, 470 uL flat coils (0° and 90°) and 5 mm bicelle coil, VT
³¹P—¹H static low-E probe, 470 uL flat coil, VT, alignment verification
¹⁹F—¹H static dual low-E probe, 470 uL flat coil, VT

Dates	PI	Submitter	Collaborators	Project/Experiment Title
11/01/09 - 11/16/09	Gan, Zhehong (FSU)	Hung, Ivan		Development of 2D solid-state NMR correlation techniques 71Ga QMAT & QPASS + QCPMG

11/17/09 - 11/22/09	Pielak, Gary (University of North Carolina-Chapel Hill)	Pielak, Gary	Fu, Riqiang	19F NMR study of synuclein -membrane interactions 19F NMR study of Synuclein -membrane interactions

11/23/09 - 11/30/09	Cross, Tim (FSU)	Sharma, Mukesh	Busath, David Fu, Riqiang Gao, Fei Li, Conggang	Solid State NMR of M2 protein Structural Studies of M2 Protein

12/01/09 -	Available	-

Research proposals and requests for instrument time on this spectrometer can be submitted online at users.magnet.fsu.edu.