NMR Program - NMR Facilities

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Specs

Designation: Imaging and Solid State NMR capabilities
Location: Tallahassee
Field: 14.1 Tesla
Bore size = 89 mm
Homogeneity = 1 ppb
RT Shims: Bruker Instruments
RT Shims ID = 72 mm
Bruker DMX console with MRI and solid state NMR capabilities
Built-in VT controller by Bruker
Amplifiers: Up to 1 kW on all channels
Gradients: Triaxis gradient for microimaging and diffusion studies, 96 G/cm max with Z-axis gradient up to 1000 G/cm
Gradients ID = 40 mm

Commercial probes

Bruker ¹H—X double resonance 4mm 15 kHz MAS probe
Bruker ¹H—(¹³C, ¹⁵N) double resonance 12 kHz MAS probe
Varian ¹H—X—Y triple resonance 6mm 9 kHz MAS probe, Y=¹⁵N...³¹P
NHMFL upper VT stack to use with above Varian probe, -150°C to +200°C
Bruker microimaging probe with 10 mm and 25 mm ¹H coils and 25 mm ¹H—³¹P coil, VT

NHMFL Low-E probes for biological solids

¹⁵N—¹H static low-E probe, 470 uL flat coils (0° and 90°) and 5 mm bicelle coil, VT
³¹P—¹H static low-E probe, 470 uL flat coil, VT, alignment verification
¹⁹F—¹H static dual low-E probe, 470 uL flat coil, VT

Dates	PI	Submitter	Collaborators	Project/Experiment Title
02/01/12 - 02/05/12	Tim Cross (FSU)	Anna Kozlova	William Brey Tim Cross Petr Gor'kov Anna Kozlova Anna Kozlova Mukesh Sharma	31P and 15N solid-state NMR study for the development of a m... 31P and 15N solid-state NMR study for the development of a m...

02/06/12 - 02/12/12	Tim Cross (FSU)	E. Vindana Ekanayake	Tim Cross E. Vindana Ekanayake E. Vindana Ekanayake Eric Rubin Mukesh Sharma	Structure Determination of LspA Using NMR 1D and 2D- CP experiment for LspA and 31P of Bicelles

02/13/12 - 02/22/12	Tim Cross (FSU)	Dylan Murray	Tim Cross Jay Griffin Dylan Murray Dylan Murray	Structure-Function Studies of Nucleotide Hydrolysis in a Mem... M. tuberculosis protein Rv1861 in aligned lipid bilayers

02/23/12 - 02/29/12	Gianluigi Veglia (University of Minnesota)	Gianluigi Veglia	Martin Gustavsson Gianluigi Veglia Gianluigi Veglia Raffaello Verardi	NMR Structural Analysis of CaATPase and Phospholamban in mem... NMR Structural Analysis of CaATPase and Phospholamban in mem...

03/01/12 -	Available	-

Research proposals and requests for instrument time on this spectrometer can be submitted online at users.magnet.fsu.edu.