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600 MHz High Resolution 52 mm NMR Magnet

SPECS:

  • Designation: Solution State NMR
  • Location: Tallahassee
  • Magnet manufacturer: Oxford Instruments
  • Field = 14.1 Tesla
  • Bore size: 52 mm
  • Homogeneity: 1 ppb
  • RT Shims: 28 channels
  • RT shims ID = 40 mm
  • RT Shims flange to COF distance = 471.2 mm +/- 1 mm
  • Console: 3-channel VARIAN Inova console with two linear full band and one linear broad band channels with 2H decoupling accessory
  • VT Control: Yes, Hi/Lo
  • Gradients: Z-axis pulsed field gradient
  • Waveforms: 3 RF channels

Users are expected to follow these rules and regulations while working on the spectrometer.  Please send your comments to Jack Skalicky.

Probe Inventory

Probe Description Tube
mm
Serial
No.
Nuclei VT Lineshape,
S/N
Pulse lengths,
Power
Varian PFG Triple 5 - 1H, 13C, 15N yes 6/10, 1200/1 8/14/40 us
Varian PFG Double 5 P000973 1H, (X=C,Si,N,P) yes 5/9, 1000/1  
Narolac PFG Triple 8 9603-2935 1H, 13C, 15N yes    

Time Schedule

DatesRequested byProject Title
05/01/08 - 05/06/08 Eisenmesser, Elan Dynamics Relaxation Experiments probing the enzyme and its s...
05/07/08 - 05/11/08 Velos, Janice CPMG D-F
05/12/08 - 05/14/08Available-
05/15/08 - 05/20/08 Eisenmesser, Elan NOESY experiments to assign cyclophilins and their CD147 rec...
05/21/08 - 05/31/08 Eisenmesser, Elan NOESY experiments to assign cyclophilins and their CD147 rec...
 06/01/08 -Available-

Research proposals and requests for instrument time on this spectrometer can be submitted online at users.magnet.fsu.edu.