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600 MHz High Resolution 52 mm NMR Magnet

SPECS:

  • Designation: Solution State NMR
  • Location: Tallahassee
  • Magnet manufacturer: Oxford Instruments
  • Field = 14.1 Tesla
  • Bore size: 52 mm
  • Homogeneity: 1 ppb
  • RT Shims: 28 channels
  • RT shims ID = 40 mm
  • RT Shims flange to COF distance = 471.2 mm +/- 1 mm
  • Console: 3-channel VARIAN Inova console with two linear full band and one linear broad band channels with 2H decoupling accessory
  • VT Control: Yes, Hi/Lo
  • Gradients: Z-axis pulsed field gradient
  • Waveforms: 3 RF channels

Users are expected to follow these rules and regulations while working on the spectrometer.  Please send your comments to Jack Skalicky.

Probe Inventory

Probe Description Tube
mm
Serial
No.
Nuclei VT Lineshape,
S/N
Pulse lengths,
Power
Varian PFG Triple 5 - 1H, 13C, 15N yes 6/10, 1200/1 8/14/40 us
Varian PFG Double 5 P000973 1H, (X=C,Si,N,P) yes 5/9, 1000/1  
Narolac PFG Triple 8 9603-2935 1H, 13C, 15N yes    

Time Schedule

Dates PI Submitter Collaborators Project/Experiment Title
10/21/09 - 11/01/09  Bruschweiler, Rafael
(NHMFL)
 Niu, Xiaogang Bruschweiler-Li, Lei
Zhang, Fengli
Protein Dynamics Research at Microsecond to Millisecond Time...
CPMG relaxation dispersion experiment

11/02/09 - 11/19/09  Eisenmesser, Elan
(University of Colorado Health Sciences Center)
 Eisenmesser, Elan   Understanding the conformational changes within the cyclophi...
N15-CPMG

11/20/09 - 11/30/09  Bruschweiler, Rafael
(NHMFL)
 Niu, Xiaogang Bruschweiler-Li, Lei
Zhang, Fengli
Protein Dynamics Research at Microsecond to Millisecond Time...
CPMG relaxation dispersion experiment

 12/01/09 - Available -

Research proposals and requests for instrument time on this spectrometer can be submitted online at users.magnet.fsu.edu.